The role of vacuum in synthetic diamonds' production
Mention diamonds and most people will associate that with the jewelry sector. They will also have in mind that such gems are to be found in
mines and sometimes won under severe conditions (โblood diamondsโ). For such reasons, the industry already investigated in the 1950s how to
produce synthetic diamonds.
Today,
there are several processes available to create artificial diamonds. Not only for jewelry where even experts are challenged to
differentiate a natural diamond from an artificial, but also for the much larger market for diamonds in the industrial sector.
Four outstanding properties of synthetic diamonds
The key properties of synthetic diamonds that make them so interesting for the industrial sector are:
Mechanical (superior hardness a chemical inertness)
Optical (high transparency)
Electrical (semiconductor properties)
Thermal (highest heat conductivity)
Some typical industrial application examples are machining and cutting tools, window material for transmitting infrared and microwave
radiation, and heat sinks for lasers and transistors. Synthetic diamonds are also the base material for semiconductor wafers and Qubits for
quantum computing.
How are diamonds obtained?
Traditionally diamonds were naturally formed billions of years ago in the earthโs crust by carbon atoms being exposed to intense heat and
pressure. However, due to technical advances, a new source of synthetically grown diamonds was created. This market can be divided into 2
main manufacturing methods:
HPHT (High-Pressure High Temperature)โ This method is based on how diamonds were naturally formed - compress carbon and add heat. The
equipment footprint often has large and limited process control.
CVD (Chemical Vapor Deposition)โ This method is based on creating a vacuum environment and then introducing specific gasses to trigger a
reaction. The equipment footprint often has a small and excellent process control.
MPCVD (Microwave Plasma CVD) growing process
Due to its small footprint and excellent process controls, the MPCVD growing process has gained in popularity. One important part of the
MPCVD process is the creation of and maintaining optimal vacuum conditions inside a growth chamber. A typical growth chamber setup looks as
below:
Close chamber and evacuate chamber for conditioning, heat up substrate
Introduce hydrogen
Turn on microwaves and generate plasma (~4000 ยฐC) above the substrate
Introduce process gases and start epitaxial growth
Methane โ carbon source
Ethanol, Acetone, or Oxygen (optional) โ helps improve the quality through oxygen plasma etching effect
Nitrogen (optional) โ helps speed up the process (learned from experience and made MPCVD growing feasible economically)
1 to 4 weeks of growth period
Which are the vacuum pump requirements for the growth period?
Initial pump down to about 2E-2 mbar base pressure
Maintain pressure (100-300 mbar, typically in a range of 100-130 mbar) while process gasses flow
Low-pressure cleanup of diamond color after production
Nowadays, oil-sealed rotary vane pumps are typically used in the MPCVD process. This is because these pumps are very well suited to
achieve low conditioning pressure but also because they are mainly designed for continuous operation at fine vacuum. Additionally, these
pumps face poor lubrication, overheating, or high oil loss when operating for days in the rough pressure phase required by this process.
Advantages of oil sealed pumps
The oil lubrication of these vacuum pumps is secured by a built-in oil pump, which also enables a uniform oil distribution at
rough pressure operation, whereas standard pumps without such oil pumps could fail.
Our range of rotary vane pumps is designed for operation at rough pressure and provides a perfect solution for the diverse pressure
requirements of this growing process:
The low ultimate pressure can easily meet the initial pump-down request, but the design of the pump also allows continuous operation at any
(even rough) operation pressure
Integrated high-efficiency exhaust filter that can reduce oil losses to the technical minimum. The oil stays inside the pump!
Compact design. There is no need for an external exhaust oil mist separator with oil return
The Ash Air range of rotary claw vacuum pumps is the best alternative to rotary vane pumps. A vacuum claw pump is virtually zero maintenance and compared to rotary vane pumps can work at vacuum levels of 400 to 1000 mbar without overheating. Rotary claw vacuum pumps are the best choice for CNC guided wood routers.
The Ash Air range of humble liquid ring pumps is still the most reliable form of large volume vacuum generation available today. These liquid ring pumps are simple to use and very reliable, and the best option when sucked air contains a large amount of saturated gas.
Dry and oil-sealed vane vacuum pumps are robust, affordable and easy in maintenance. You can use DVP vane pumps for wide range of application, for skin packaging, holding, lifting, thermoforming.
We have a great range of new and hire blowers from single stage ring blower through to large lobe blowers, and we also stock the service parts for common blowers across many brands.
Our roots blowers, side channel blowers are built to last, and are backed up by our promise of excellent customer service to keep your business performing well day in and day out.
With hundreds of years of combined experience and a broad product range, Ash Air is a great partner for your vacuum pump operations.
From rotary vane pumps to screw pumps and accessories, we have a large variety of products. We also have a dedicated
applications team ready to calculate the ideal pump configuration. With a global support organization, we can support your manufacturing
operations wherever they may be located in New Zealand.
Do you have an idea for our #expertcorner?ย Let
us know!
Who we are and how Ash Air can help your business!
Ash Air has been around in New Zealand since 1979, and weโve grown into a nationwide company with international support and a
reputation for quality and reliability.We look after all things compressed air for your business!
Reciprocating, Screw, air compressors
Vacuum pumps
Nitrogen
An extensive line of air treatment components
Ash Air's range of Chicago Pneumatic, Alup, Pneumatech, and Quincy compressors are used extensively around the world in industries
ranging from oil and gas to food, automotive and farming, and we bring you these world class compressors here in the land of the long white
cloud.Our technicians are compressed air equipment experts and are dedicated to addressing customer needs. Supported by a 13 locations
nationwide, Ash Air offers one of the widest selections of compressed air equipment and parts available today in New Zealand.
Reliability and Efficiency
With Ash Air compressors, you can count on reliability and high performance for even the most demanding applications. We focus our
efforts on the following:
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